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Beilstein J. Org. Chem. 2019, 15, 721–726, doi:10.3762/bjoc.15.67
Graphical Abstract
Scheme 1: Synthesis of 4,5-dihydroisobenzofuran-5-ol (3).
Scheme 2: Protection strategy of 4,5-dihydroisobenzofuran-5-ol (3).
Scheme 3: Oxidation of 5-substituted-4,5-dihydroisobenzofuran-5-ol in presence of SeO2 or DDQ.
Scheme 4: Synthesis of 4-hydroxy-ortho-phthalaldehyde (6) through MAOS demethylation of 4-methoxy-ortho-phtha...
Beilstein J. Org. Chem. 2015, 11, 2785–2794, doi:10.3762/bjoc.11.299
Scheme 1: Schematic representation of molecular imprinting technique. i) Polymerization process with toluene-...
Figure 1: FTIR spectra of (A): native CRYSMEB, (B): D3 (toluene/CD 3:1), (C): D2 (toluene/CD 4:1), and (D): D...
Figure 2: Top: XRPD pattern for CRYSMEB. Bottom: XRPD pattern for D1 polymer. The diffraction peaks denoted w...
Figure 3: 13C {1H} CP-MAS spectra of polymers D1, D2 and D3. Peak assignment is given in the upper trace.
Figure 4: 13C {1H} CP-MAS spectra of native CRYSMEB and polymer D3. Peak assignment is given on CRYSMEB spect...
Figure 5: 1D 13C CP/MAS spectra of polymer D3 as a function of the contact time varying from 35 μs to 4 ms.
Figure 6: Cross-polymerization (CP) build-up curve of the 13C resonances with variable contact times for the ...
Figure 7: Cross-polymerization (CP) build-up curve of the 13C resonances with variable contact time for polym...
Figure 8: CP build-up curves of the 13C resonances with cross-polymerization in the range 0–100 μs for polyme...